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A regioselective direct alkylation of coumarins at C-3 via cross-dehydrogenative coupling of unactivated Csp 2–Csp 3 bonds is developed. This protocol employs tert-butyl hydroperoxide as the sole reagent of the reaction to combine coumarins and ethers in reasonable yields under metal- and solvent-free reaction conditions. Download game bola ukuran kecil untuk pc.
This protocol also worked well with coumarin-3-carboxylic acids to unveil a rare instance of a catalyst-free tandem alkylation/decarboxylation reaction with conservation of the double bond. For reproduction of material from NJC: Reproduced from Ref. XX with permission from the Centre National de la Recherche Scientifique (CNRS) and The Royal Society of Chemistry. For reproduction of material from PCCP: Reproduced from Ref. XX with permission from the PCCP Owner Societies. For reproduction of material from PPS: Reproduced from Ref.
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XX with permission from the European Society for Photobiology, the European Photochemistry Association, and The Royal Society of Chemistry. For reproduction of material from all other RSC journals and books: Reproduced from Ref. XX with permission from The Royal Society of Chemistry. If the material has been adapted instead of reproduced from the original RSC publication 'Reproduced from' can be substituted with 'Adapted from'. In all cases the Ref. XX is the XXth reference in the list of references. If you are the author of this article you do not need to formally request permission to reproduce figures, diagrams etc.
Contained in this article in third party publications or in a thesis or dissertation provided that the correct acknowledgement is given with the reproduced material. Reproduced material should be attributed as follows.
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